HCID 22345612, compound → HCID 22345640, compound

HRID 584297Notes

Reaction equation

HRID 584297 reaction equation
[Si]([O:8][C:9]1[CH:14]=[CH:13][C:12]([C:15](=[O:18])[CH2:16][CH3:17])=[CH:11][C:10]=1[CH2:19][CH3:20])(C(C)(C)C)(C)C>C1COCC1>[CH2:19]([C:10]1[CH:11]=[C:12]([C:15](=[O:18])[CH2:16][CH3:17])[CH:13]=[CH:14][C:9]=1[OH:8])[CH3:20]

Participants

3

Reactant 1

HCID 22345612HCID 22345612, compound

Product 1

HCID 22345640HCID 22345640, compoundYield 100%

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

In a manner similar to that of Example 1(m), starting with 6.8 g (23 mmol) of 1-[4-(tert-butyldimethylsilanyloxy)-3-ethylphenyl]propan-1-one in 50 ml of THF, 4.1 g (100%) of the expected product are obtained in the form of a beige-colored oil.

Sources & evidence

ORD record
ord-552ba7b03a6146d9984fc353730c4277
Source dataset
uspto-grants-2005_08
Patent number
US06924400B2

Reaction notes

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