HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4-Bis(benzoyloxymethyl)benzyl bromide → 1-{5'-[3,4-Bis(benzoyloxymethyl)benzyloxy]-2'-ethyl-2-propylbiphenyl-4-yl}-1-propan-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4-Bis(benzoyloxymethyl)benzyl bromide | HCID 22345618 | — |
| Reactant | 1-(2'-Ethyl-5'-hydroxy-2-propylbiphenyl-4-yl)-1-propanone | HCID 22345639 | — |
| Product | 1-{5'-[3,4-Bis(benzoyloxymethyl)benzyloxy]-2'-ethyl-2-propylbiphenyl-4-yl}-1-propan-one | HCID 22345607 | — |
Reaction Steps
In a manner similar to that of Example 1(o), by reacting 1.28 g (4.3 mmol) of 1-(2′-ethyl-5′-hydroxy-2-propylbiphenyl-4-yl)-1-propanone with 1.98 g (4.5 mmol) of 3,4-bis(benzoyloxymethyl)benzyl bromide, an oil is obtained, which is used without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06924400B2 |
| Source dataset | uspto-grants-2005_08 |
| ORD ID | ord-5d9d94cadcb047298a98500f0693977a |
| Source note | uspto-grants-2005_08 |