HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4-Bis(benzoyloxymethyl)benzyl bromide → 1-{5'-[3,4-Bis(benzoyloxymethyl)benzyloxy]-2'-ethyl-2-isopropylbiphenyl-4-yl}-1-propanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4-Bis(benzoyloxymethyl)benzyl bromide | HCID 22345618 | — |
| Reactant | 1-(2'-Ethyl-5'-hydroxy-2-isopropylbiphenyl-4-yl)propan-1-one | HCID 22345623 | — |
| Product | 1-{5'-[3,4-Bis(benzoyloxymethyl)benzyloxy]-2'-ethyl-2-isopropylbiphenyl-4-yl}-1-propanone | HCID 22345613 | — |
Reaction Steps
In a manner similar to that of Example 1(o), by reacting 660 mg (2.2 mmol) of 1-(2′-ethyl-5′-hydroxy-2-isopropylbiphenyl-4-yl)propan-1-one with 1 g (2.3 mmol) of 3,4-bis-(benzoyloxymethyl)benzyl bromide, an oil is obtained, which is used without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06924400B2 |
| Source dataset | uspto-grants-2005_08 |
| ORD ID | ord-05ef296bdc604a86bd05cce7bc87993b |
| Source note | uspto-grants-2005_08 |