HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 9907539, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Ethyl 3-bromopropionate | HCID 68320 | — |
| Reactant | HCID 178439934 | HCID 178439934 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 9907539 | HCID 9907539 | — |
Reaction Steps
To a solution of 6,7-dichloro-3-isopropylquinoxaline-2-thiol (36 mg, 0.13 mmol) in DMF was added potassium carbonate (55 mg, 0.40 mmol) followed by ethyl 3-bromopropionate (0.02 ml, 0.16 mmol). The reaction was stirred at room temperature for 4 days. Purification by flash column chromatography using ethyl acetate:hexanes 1:40 afforded the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06927214B1 |
| Source dataset | uspto-grants-2005_08 |
| ORD ID | ord-8ef5925c10404b01aecd7b6dafd3f8a4 |
| Source note | uspto-grants-2005_08 |