Methanesulfinic acid → HCID 22341189, compound

Participants

Reaction Steps

To a solution of 3-chloromethyl-2,6,7-trichloroquinoxaline (150 mg, 0.53 mmol) in DMF (3 ml) was added methanesulfinic acid, sodium salt (120 mg, 1.06 mmol). The reaction mixture was stirred at room temperature overnight. The solvent was removed and the residue was purified by column chromatography (ethyl acetate:hexane 1:2) to afford the title compounds as a white solid.

Provenance & Evidence