HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lawesson's reagent → HCID 60024140, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lawesson's reagent | HCID 87949 | — |
| Reactant | HCID 60024116 | HCID 60024116 | — |
| Product | HCID 60024140 | HCID 60024140 | — |
Reaction Steps
Following the procedure described in Example 1 for the preparation of 1 the reaction of 15 with Lawesson's Reagent provides the title compound (13), which is purified by silica gel chromatography with 2.5% MeOH—CH2Cl2 and crystallization from EtOAc-hexane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06927229B2 |
| Source dataset | uspto-grants-2005_08 |
| ORD ID | ord-12a8b1d60a1e407c870562005b6a3fb8 |
| Source note | uspto-grants-2005_08 |