HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → HCID 22341459, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | HCID 10157037 | HCID 10157037 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 22341459 | HCID 22341459 | — |
Reaction Steps
By reacting 1.6 g (4.1 mmol) of 2-methyl-3-(3′-{[methyl-(1-phenylmethanoyl)amino]methyl}biphenyl-4-yl)propionic acid with 390 μl (4.5 mmol) of oxalyl chloride in dichloromethane, and after evaporation, 1.7 g (100%) of 3-(3′-{[methyl-(1-phenylmethanoyl)-amino]methyl}biphenyl-4-yl)propionyl chloride are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06927228B2 |
| Source dataset | uspto-grants-2005_08 |
| ORD ID | ord-61cd9081043c4ba5be44c4caa783a085 |
| Source note | uspto-grants-2005_08 |