HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69792650, compound → HCID 69792812, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69792650 | HCID 69792650 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 69792812 | HCID 69792812 | 77.1% |
Reaction Steps
In a manner similar to that of Example 1(g), starting with 1.70 g (3.5 mmol) of methyl ethyl 2-{3′-[(heptanoylmethylamino)methyl]biphenyl-4-ylmethylene}succinate and 170 mg (10% by mass) of 10% palladium-on-charcoal in 20 ml of ethyl acetate, 1.30 g (77%) of the expected product are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06927228B2 |
| Source dataset | uspto-grants-2005_08 |
| ORD ID | ord-ab830c4f12e549299801950e0ccf346c |
| Source note | uspto-grants-2005_08 |