HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 73884093, compound → HCID 22341454, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 73884093 | HCID 73884093 | — |
| Solvent | Dioxane Methanol | HCID 21966525 | — |
| Product | HCID 22341454 | HCID 22341454 | — |
Reaction Steps
In a manner similar to that of Example 1(g), starting with 3 g (10.1 mmol) of 5-(3′-hydroxybiphenyl-4-ylmethylene)thiazolidine-2,4-dione in a dioxane/methanol mixture (50/50), and after purification by chromatography on a column of silica eluted with a heptane/ethyl acetate mixture (7/3), 800 mg (27%) of the expected product are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06927228B2 |
| Source dataset | uspto-grants-2005_08 |
| ORD ID | ord-6285a2c4acd744a2a29bbdb6a71538d3 |
| Source note | uspto-grants-2005_08 |