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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 584987Generated: October 30, 2026

HCID 73884093, compound → HCID 22341454, compound

https://huagongshe.com/reaction/584987

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 73884093HCID 73884093—
SolventDioxane MethanolHCID 21966525—
ProductHCID 22341454HCID 22341454—

Reaction Steps

In a manner similar to that of Example 1(g), starting with 3 g (10.1 mmol) of 5-(3′-hydroxybiphenyl-4-ylmethylene)thiazolidine-2,4-dione in a dioxane/methanol mixture (50/50), and after purification by chromatography on a column of silica eluted with a heptane/ethyl acetate mixture (7/3), 800 mg (27%) of the expected product are obtained.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06927228B2
Source datasetuspto-grants-2005_08
ORD IDord-6285a2c4acd744a2a29bbdb6a71538d3
Source noteuspto-grants-2005_08