HuagongsheHuagongshe Chemistry Print Report · For research reference only
Octanoyl chloride → HCID 22341412, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Octanoyl chloride | HCID 8124 | — |
| Reactant | 3-Bromo-N-methyl-4-(phenylmethoxy)benzenemethanamine | HCID 17157577 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 22341412 | HCID 22341412 | 98.3% |
Reaction Steps
In a manner similar to that of Example 37(e), by reacting 9.9 g (32 mmol) of N-(4-benzyloxy-3-bromo benzyl)-N-methylamine with 5.3 g (32 mmol) of octanoyl chloride in 90 ml of dichloromethane, 13.6 g (97%) of the expected product are obtained in the form of a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06927228B2 |
| Source dataset | uspto-grants-2005_08 |
| ORD ID | ord-9496eabcfa874050b030b0f8d46ef0d6 |
| Source note | uspto-grants-2005_08 |