Octanoyl chloride → HCID 22341492, compound

Participants

Reaction Steps

In a manner similar to that of Example 37(e), by reacting 6 g (19.6 mmol) of N-(2-benzyloxy-5-bromo benzyl)-N-methylamine with 3.4 ml (19.6 mmol) of octanoyl chloride, and after purification by chromatography on a column of silica eluted with a heptane/ethyl acetate mixture (8/2), 8 g (95%) of the expected product are obtained in the form of a colorless oil.

Provenance & Evidence