HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-formyl-1-aminoundec-10-ene → N-Undecylformamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-formyl-1-aminoundec-10-ene | HCID 12039861 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | N-Undecylformamide | HCID 268113 | 100% |
Reaction Steps
N-formyl-1-aminoundec-10-ene (467 mg) was dissolved in ethanol (2 ml). Pd/C (46 mg) was added and the mixture submitted to hydrogenation at atmospheric pressure during 10 h. The reaction mixture was filtered through a short column of celite and the solvent evaporated under vacuo. This yielded N-formyl-1-aminoundecane (468 mg, yield: 100%) as a white solid
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06929685B2 |
| Source dataset | uspto-grants-2005_08 |
| ORD ID | ord-de7c52b32cb441e2b73bdf3b79102a6d |
| Source note | uspto-grants-2005_08 |