HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Methoxide → HCID 86759813, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | HCID 12149031 | HCID 12149031 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 86759813 | HCID 86759813 | — |
Reaction Steps
Compound 18 (1.57 g) was suspended in methanol (30 mL), and sodium methoxide was added to the resultant mixture until an substantially homogeneous solution was obtained. The solution was filtered, and the filtrate was concentrated. Diethyl ether was added thereto, and the resultant colorless crystals were collected through filtration and dried under reduced pressure, to thereby yield 1.57 g of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06933309B2 |
| Source dataset | uspto-grants-2005_08 |
| ORD ID | ord-6a72eb87892042ac8342630520857dfa |
| Source note | uspto-grants-2005_08 |