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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 585730Generated: October 31, 2026

Sodium borohydride → HCID 20824481, compound

https://huagongshe.com/reaction/585730

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSodium borohydrideHCID 4311764—
ReactantHCID 20824482HCID 20824482—
ProductHCID 20824481HCID 2082448198%

Reaction Steps

By a similar reaction operation as in Starting Material Synthetic Example 1 using 5-oxo-2,3,4,5-tetrahydro-1-benzothiepine-8-carboxylic acid methyl ester (3.30 g) and sodium borohydride (529 mg), the objective 5-hydroxy-2,3,4,5-tetrahydro-1-benzothiepine-8-carboxylic acid methyl ester (3.26 g) was obtained a pale yellow oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06933305B2
Source datasetuspto-grants-2005_08
ORD IDord-206d5e5e053b4761bc2f729d9d760813
Source noteuspto-grants-2005_08