HuagongsheHuagongshe Chemistry Print Report · For research reference only
6,6-Dimethyl-5,7-dioxaspiro(2.5)octane-4,8-dione → HCID 66832065, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6,6-Dimethyl-5,7-dioxaspiro(2.5)octane-4,8-dione | HCID 79720 | — |
| Reactant | 3-(1H-pyrrol-1-yl)aniline | HCID 2760546 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 66832065 | HCID 66832065 | 80% |
Reaction Steps
This compound was prepared according to general method 1 starting from 6,6-dimethyl-5,7-dioxaspiro[2.5]octane-4,8-dione (0.250 g, 1.47 mmol) and 3-(1H-pyrrol-1-yl)aniline (0.697 g; 4.41 mmol) in ethanol (3 mL). 1-(3-(1H-pyrrol-1-yl)phenyl)-2-oxopyrrolidine-3-carboxylic acid 0.313 g (80%) was obtained as a brown oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09434722B2 |
| Source dataset | uspto-grants-2016_09 |
| ORD ID | ord-6ec33ae0a78f412e9339409783ff247a |
| Source note | uspto-grants-2016_09 |