Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Bis(neopentyl glycolato)diboron → 4-Fluoro-3-([1,2,4]triazol-1-yl)phenylboronic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Bis(neopentyl glycolato)diboron | HCID 2734316 | — |
| 반응물 | 1-(5-Bromo-2-fluorophenyl)-1h-[1,2,4]triazole | HCID 22329542 | — |
| 생성물 | 4-Fluoro-3-([1,2,4]triazol-1-yl)phenylboronic acid | HCID 22329489 | — |
반응 단계
1-(5-Bromo-2-fluorophenyl)-1H-[1,2,4]triazole (1.1 g, 4.5 mmol) was reacted with bis(neopentyl glycolato)diboron (1.13 g, 5.0 mmol) using the method in Example 49 to give 4-fluoro-3-([1,2,4]triazol-1-yl)phenylboronic acid as a white solid: MS (ES+) m/z 208 [M+H]+.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06936608B2 |
| 출처 데이터셋 | uspto-grants-2005_08 |
| ORD ID | ord-0b1efe95fb4345a696d7b41555c1fe54 |
| 출처 메모 | uspto-grants-2005_08 |