7-Bromo-3-trifluoromethyl-imidazo[1,2-B][1,2,4]triazine → HCID 10269265、化合物

関与物質

役割	名称	HCID	仕込み量
反応物	7-Bromo-3-trifluoromethyl-imidazo[1,2-B][1,2,4]triazine	HCID 11601416	—
反応物	4-Fluoro-3-([1,2,4]triazol-1-yl)phenylboronic acid	HCID 22329489	—
生成物	HCID 10269265	HCID 10269265	—

反応手順

7-Bromo-3-trifluoromethylimidazo[1,2-b][1,2,4]triazine was coupled with 4-fluoro-3-([1,2,4]triazol-1-yl)phenylboronic acid as described in Example 3, step f, final paragraph, to give the title compound: 1H NMR (360 MHz, DMSO-d6) δ 7.82 (1H, dd, J 8.7, 10.5 Hz), 8.34-8.39 (1H, m), 8.39 (1H, s), 8.71 (1H, dd, J 2.4, 7.4 Hz), 9.02 (1H, s), 9.13 (1H, d, J 2.4 Hz); MS (ES+) m/z 350 [M+H]+.

情報源と証拠

DOI	10.6084/m9.figshare.5104873.v1
特許番号	US06936608B2
出典データセット	uspto-grants-2005_08
ORD ID	ord-311be3471d0f491cbfa35335f64b9911
出典メモ	uspto-grants-2005_08