Hydrochloric Acid → HCID 22262525, compound

HRID 586563Notes

Reaction equation

HRID 586563 reaction equation
C([NH:20][CH2:21][CH2:22][NH:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][NH:30][CH2:31][CH2:32][NH:33]C(C1C=CC=CC=1)(C1C=CC=CC=1)C1C=CC=CC=1)(C1C=CC=CC=1)(C1C=CC=CC=1)C1C=CC=CC=1.[ClH:53]>>[ClH:53].[ClH:53].[ClH:53].[ClH:53].[NH2:33][CH2:32][CH2:31][NH:30][CH2:29][CH2:28][CH2:27][CH2:26][CH2:25][CH2:24][NH:23][CH2:22][CH2:21][NH2:20]

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 22262526HCID 22262526, compound

Product 1

HCID 22262525HCID 22262525, compound

Procedure

A mixture of N, N′-bis(2′-tritylaminoethyl)-1,6-diaminohexane (1.0 g 1.45 mmol) and 6 M HCl (30 ml) was refluxed for 3 h. The mixture was filtered and the filtrate was concentrated to about 3 ml over vacuao. Addition of methanol into the concentrated solution afforded a white salt.

Workup

  1. temperaturewas refluxed for 3 h
  2. filtrationThe mixture was filtered
  3. concentrationthe filtrate was concentrated to about 3 ml over vacuao
  4. additionAddition of methanol into the concentrated solution
  5. customafforded a white salt

Sources & evidence

ORD record
ord-c2f6462f920f4616912a49dc22bd0465
Source dataset
uspto-grants-2005_08
Patent number
US06936634B2

Reaction notes

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