Iodoethane → HCID 69737497, compound

HRID 586679Notes

Reaction equation

HRID 586679 reaction equation
[CH3:1][O:2][CH2:3][CH:4]1[C@@H:6]([CH2:7][OH:8])[C:5]1([CH3:21])[C:9]1[CH:14]=[C:13]([CH:15]([CH3:17])[CH3:16])[CH:12]=[C:11]([CH:18]([CH3:20])[CH3:19])[CH:10]=1.[CH2:22](I)C>>[CH2:1]([O:2][CH2:3][CH:4]1[C@H:6]([CH2:7][OH:8])[C:5]1([CH3:21])[C:9]1[CH:10]=[C:11]([CH:18]([CH3:20])[CH3:19])[CH:12]=[C:13]([CH:15]([CH3:16])[CH3:17])[CH:14]=1)[CH3:22]

Participants

3

Reactant 2

HCID 6340IodoethaneHCID 69723272HCID 69723272, compound

Product 1

HCID 69737497HCID 69737497, compoundYield 77%

Procedure

Following a procedure similar to that for the preparation of Intermediate 39 but using Intermediate 38 as the starting material and ethyl iodide as alkylating reagent yielded the title compound (89 mg, 77% yield) as a colorless oil:

Sources & evidence

ORD record
ord-46c209467f3d4621b1d83cc50ed6f342
Source dataset
uspto-grants-2005_08
Patent number
US06936636B2

Reaction notes

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