HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Benzylpiperazine → HCID 4314202, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Benzylpiperazine | HCID 75994 | — |
| Reactant | 2-Fluoro-5-nitrobenzonitrile | HCID 519417 | — |
| Product | HCID 4314202 | HCID 4314202 | 89% |
Reaction Steps
The experimental protocol used is the same as that described for compound 6.1, 2-fluoro-5-nitrobenzonitrile replacing 2-fluoro-5-nitrotoluene and 1-benzylpiperazine replacing tert-butyl 1-piperazinecarboxylate. A light ochre-coloured solid is obtained (yield 89%). Melting point: 124.0° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06936715B2 |
| Source dataset | uspto-grants-2005_08 |
| ORD ID | ord-a630b08417e94dee87c927206adfd1ef |
| Source note | uspto-grants-2005_08 |