HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22335453, compound → HCID 131725107, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22335453 | HCID 22335453 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 131725107 | HCID 131725107 | 199.6% |
Reaction Steps
The product from example 13 (50 mg, 0.0635 mmol) was treated with trifluoacetic acid (2.0 mL) in dichloromethane (2.0 mL) at rt for 1 h. The mixture was concentrated in vacuo to provide the title barbituric acid (50.8 mg, 100%). MS found: (M+H)+=460.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06936620B2 |
| Source dataset | uspto-grants-2005_08 |
| ORD ID | ord-2475f9afd6654763960f4e4fc7426ba4 |
| Source note | uspto-grants-2005_08 |