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HRID587141

反应详情

EQUATION

反应方程式

HRID 587141 的结构方程式

REACTANTS

反应物

3
结构：COCC1CCCCN1.Cl
HCID45926159

未命名化合物

结构：NS(=O)(=O)Cc1cccc(Nc2ncnc(N3CCC(F)(F)CC3)n2)c1
HCID60197102

未命名化合物

结构：NS(=O)(=O)Cc1cccc(Nc2ncnc(Cl)n2)c1
HCID86679822

未命名化合物

PRODUCTS

生成物

1
结构：COCC1CCCCN1c1ncnc(Nc2cccc(CS(N)(=O)=O)c2)n1
HCID60197106

未命名化合物

PROCEDURE

实验过程

B4 was prepared following the procedure reported for B2 using A1 and rac-2-methoxymethylpiperidine hydrochloride. The title compound was purified by thick-layer chromatography (silica gel, chloroform/MeOH 19:1) and obtained as a white crystalline solid; yield: 235 mg (67%). MS (ES) C17H24N6O3S requires: 392. found: 393 (M+H)+.

WORKUP

后处理

  1. customThe title compound was purified by thick-layer chromatography (silica gel, chloroform/MeOH 19:1)
  2. customobtained as a white crystalline solid