Diethyl Sulfate → HCID 59419917, compound

HRID 587919Notes

Reaction equation

[CH3:1][O:2][C:3](=[O:15])[CH2:4][C:5]1[CH:10]=[CH:9][C:8]([O:11][CH3:12])=[C:7]([O:13][CH3:14])[CH:6]=1.COC1C=[C:20]([CH2:26][C:27]#N)C=CC=1OC.S(O[CH2:36][CH3:37])(OCC)(=O)=O.[Br:38]C(C)C>>[Br:38][CH2:27][CH2:26][CH2:20][C:4]([C:5]1[CH:10]=[CH:9][C:8]([O:11][CH3:12])=[C:7]([O:13][CH3:14])[CH:6]=1)([CH2:36][CH3:37])[C:3]([O:2][CH3:1])=[O:15]

Participants

Reactant 4

HCID 6163Diethyl Sulfate

HCID 63582-Bromopropane

HCID 667273,4-Dimethoxybenzeneacetonitrile

HCID 85213Benzeneacetic acid, 3,4-dimethoxy-, methyl ester

Product 1

HCID 59419917HCID 59419917, compound

Procedure

For Step 1, (3,4-dimethoxy-phenyl)-acetic acid methyl ester was substituted for (3,4-Dimethoxyphenyl)acetonitrile and diethyl sulfate was substituted for 2-bromopropane.

Sources & evidence

ORD record: ord-9a7d1553640440849cc4cbcf038f31fd
Source dataset: uspto-grants-2016_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US09227918B2

Reaction notes

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