Diethyl Sulfate → HCID 59419919, compound

HRID 587920Notes

Reaction equation

HRID 587920 reaction equation
[CH2:1]([O:3][C:4](=[O:16])[CH2:5][C:6]1[CH:11]=[CH:10][C:9]([O:12][CH3:13])=[C:8]([O:14][CH3:15])[CH:7]=1)[CH3:2].COC1C=[C:21]([CH2:27][C:28]#N)C=CC=1OC.S(O[CH2:37][CH3:38])(OCC)(=O)=O.[Br:39]C(C)C>>[Br:39][CH2:28][CH2:27][CH2:21][C:5]([C:6]1[CH:11]=[CH:10][C:9]([O:12][CH3:13])=[C:8]([O:14][CH3:15])[CH:7]=1)([CH2:37][CH3:38])[C:4]([O:3][CH2:1][CH3:2])=[O:16]

Participants

5

Reactant 4

HCID 6163Diethyl SulfateHCID 63582-BromopropaneHCID 667273,4-DimethoxybenzeneacetonitrileHCID 87441Ethyl 3,4-dimethoxyphenylacetate

Product 1

HCID 59419919HCID 59419919, compound

Procedure

For Step 1, (3,4-dimethoxy-phenyl)-acetic acid ethyl ester was substituted for (3,4-Dimethoxyphenyl)acetonitrile and diethyl sulfate was substituted for 2-bromopropane.

Sources & evidence

ORD record
ord-17282a173cdb42e3b6bc42ba87783dc9
Source dataset
uspto-grants-2016_01
Patent number
US09227918B2

Reaction notes

Loading…