HRID587990

反应详情

EQUATION

反应方程式

HRID 587990 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Imidazole (43.2 g, 635 mmol) was dissolved in tetrahydrofuran (100 ml), and under ice cooling, thionyl chloride (23.5 g, 199 mmol) was added thereto. The reaction mixture was stirred for 3 hours at room temperature, and then the salt thus produced was separated by filtration. Thus, a sulfinyldiimidazole solution was obtained.

WORKUP

后处理

  1. customthe salt thus produced
  2. customwas separated by filtration