HuagongsheHuagongshe Chemistry Print Report · For research reference only
(4-Aminophenoxy)benzene → HCID 71496600, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (4-Aminophenoxy)benzene | HCID 8764 | — |
| Reactant | 1-Benzyl-4-piperidylamine | HCID 415852 | — |
| Reactant | HCID 1419048 | HCID 1419048 | — |
| Reactant | HCID 4548294 | HCID 4548294 | — |
| Product | HCID 71496600 | HCID 71496600 | 77.8% |
Reaction Steps
The title compound was prepared in the same manner as in Example 1, with the exception that 2-chloro-(N-4-phenoxyphenyl)nicotinamide of Preparation Example 6, instead of 2-chloro-(N-3-chlorophenyl)nicotinamide, and 4-phenoxyaniline, instead of 4-amino-1-benzylpiperidine, were used in the same molar amounts (Yield: 77.8%). 1H NMR (DMSO-d6) δ 10.50 (s, 1H), 10.33 (s, 1H), 8.35 (d, 1H), 8.25 (d, 1H), 7.69˜7.82 (m, 4H), 7.30˜7.46 (m, 4H), 6.88˜7.18 (m, 11H) ppm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09227955B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-ca9c723f1d634a71b4e5c7b50d7eca7c |
| Source note | uspto-grants-2016_01 |