Diethylamine → (6-Bromo-[1,2,4]triazolo[1,5-a]pyridin-2-yl)-diethyl-amine

HRID 588450Notes

Reaction equation

HRID 588450 reaction equation
C(NCC)C.[Br:6][C:7]1[CH:8]=[CH:9][C:10]2[N:11]([N:13]=[C:14]([N:16]3[CH2:21][CH2:20]O[CH2:18][CH2:17]3)[N:15]=2)[CH:12]=1>>[Br:6][C:7]1[CH:8]=[CH:9][C:10]2[N:11]([N:13]=[C:14]([N:16]([CH2:21][CH3:20])[CH2:17][CH3:18])[N:15]=2)[CH:12]=1

Participants

3

Reactant 2

HCID 8021DiethylamineHCID 717438774-(6-Bromo-[1,2,4]triazolo[1,5-A]pyridin-2-YL)morpholine

Product 1

HCID 89464394(6-Bromo-[1,2,4]triazolo[1,5-a]pyridin-2-yl)-diethyl-amine

Procedure

Using diethylamine, this compound was prepared following the same method as for the synthesis of 6-bromo-2-morpholin-4-yl-[1,2,4]triazolo[1,5-a]pyridine Light brown solid (2.0 g, 82%). MS: m/z=270 (M+H+).

Workup

  1. customthis compound was prepared

Sources & evidence

ORD record
ord-3c7ca0af60fe4217bd72d309c74da5a8
Source dataset
uspto-grants-2016_01
Patent number
US09227970B2

Reaction notes

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