HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Iodosuccinimide → CID 86717264
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Iodosuccinimide | HCID 120273 | — |
| Reactant | 4-chloro-5-phenyl-1H-pyrazolo[3,4-c]pyridazine | HCID 86717263 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | CID 86717264 | HCID 86717264 | — |
Reaction Steps
A suspension of 4-chloro-5-phenyl-1H-pyrazolo[3,4-c]pyridazine (2.44 g, 10.6 mmol) and N-iodosuccinimide (3.58 g, 15.9 mmol) in acetonitrile (106 mL) was heated at reflux for 1 d. The yellow solid was collected by filtration whilst warm to provide a mixture of the title compound and starting material (9:1, 4 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09227976B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-6315fa9e8ee64983b46b55d62701630f |
| Source note | uspto-grants-2016_01 |