反应详情

温度

70 °C

A mixture of 9 g of methyl 3-(3-cyclohexenyl)-5chlorosalicylate and 20 ml trifluoroacetic acid is heated at 70° C. overnight. The cooled reaction mixture is diluted with hexanes, washed three times with water, dried and evaporated to dryness. The residue is purified with flash chromatography using 10% ethyl acetate/hexane to give four fractions

1. customThe cooled reaction mixture
2. washwashed three times with water
3. customdried
4. customevaporated to dryness
5. customThe residue is purified with flash chromatography
6. customto give four fractions