HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nitric Acid → HCID 90410240, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nitric Acid | HCID 944 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | 2-Bromo-4-fluoro-5-nitrophenol | HCID 13268179 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 90410240 | HCID 90410240 | — |
Reaction Steps
To a solution of 2-bromo-4-fluoro-5-nitrophenol (4.0 g, 17 mmol) in methylene chloride (29.5 mL), 2.0 M nitric acid in DCM (25 mL) was added and the mixture was stirred for 15 min at room temperature. The mixture was poured over cold water and extracted with methylene chloride to give the product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09227985B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-7fcf471009b9404c90fdba0c7e9bf2ee |
| Source note | uspto-grants-2016_01 |