HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 67294821, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Benzyl chloroformate | HCID 10387 | — |
| Reactant | 1-(5-Bromopyridin-2-yl)cyclopropanamine | HCID 57356818 | — |
| Product | HCID 67294821 | HCID 67294821 | — |
Reaction Steps
At 0° C., to the mixture of 1-(5-bromopyridin-2-yl)cyclopropanamine (1.07 g, 5.0 mmol), triethylamine (766 ul, 5.5 mmol) was added benzyl chloroformate (785 ul, 5.5 mmol). The resulting mixture was allowed to stir at it for 1 h. After work up, the crude product was purified by column chromatography on SiO2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09227971B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-387dd3a1ae514f7eba8594e703581027 |
| Source note | uspto-grants-2016_01 |