HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropylamine → Isopropylammonium 5-(trifluoromethyl)benzo[b]thiophene-2-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropylamine | HCID 6363 | — |
| Reactant | 5-(Trifluoromethyl)-1-benzothiophene-2-carboxylic acid | HCID 2783043 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | Isopropylammonium 5-(trifluoromethyl)benzo[b]thiophene-2-carboxylate | HCID 70982169 | 100% |
Reaction Steps
A mixture of 300 mg of 5-(trifluoromethyl)benzo[b]thiophene-2-carboxylic acid, 80 mg of isopropylamine and 10 ml of tetrahydrofuran was stirred at room temperature for 1 hour. The reaction mixture was concentrated under reduced pressure to obtain 372 mg of isopropylammonium 5-(trifluoromethyl)benzo[b]thiophene-2-carboxylate (hereinafter referred to as “the present compound 7”).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09232792B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-c77e20fb3ae54471a8f6780dc5f15fec |
| Source note | uspto-grants-2016_01 |