HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dodecylamine → Laurylammonium 5-(trifluoromethyl)benzo[b]thiophene-2-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dodecylamine | HCID 13583 | — |
| Reactant | 5-(Trifluoromethyl)-1-benzothiophene-2-carboxylic acid | HCID 2783043 | — |
| Solvent | tert-Butyl methyl ether | HCID 15413 | — |
| Product | Laurylammonium 5-(trifluoromethyl)benzo[b]thiophene-2-carboxylate | HCID 70982284 | 102.3% |
Reaction Steps
A mixture of 300 mg of 5-(trifluoromethyl)benzo[b]thiophene-2-carboxylic acid, 238 mg of laurylamine and 10 ml of tert-butyl methyl ether was stirred at room temperature for 1 hour. The reaction mixture was concentrated under reduced pressure to obtain 538 mg of laurylammonium 5-(trifluoromethyl)benzo[b]thiophene-2-carboxylate (hereinafter referred to as “the present compounds 8”).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09232792B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-09e727217a354c048c071e408deddb07 |
| Source note | uspto-grants-2016_01 |