HRID589290

反应详情

EQUATION

反应方程式

HRID 589290 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A mixture of 300 mg of 5-(trifluoromethyl)benzo[b]thiophene-2-carboxylic acid, 238 mg of laurylamine and 10 ml of tert-butyl methyl ether was stirred at room temperature for 1 hour. The reaction mixture was concentrated under reduced pressure to obtain 538 mg of laurylammonium 5-(trifluoromethyl)benzo[b]thiophene-2-carboxylate (hereinafter referred to as “the present compounds 8”).

WORKUP

后处理

  1. concentrationThe reaction mixture was concentrated under reduced pressure