HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzaldehyde → 2-(Benzylideneamino)phenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzaldehyde | HCID 240 | — |
| Reactant | 2-Aminophenol | HCID 5801 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 2-(Benzylideneamino)phenol | HCID 219809 | — |
Reaction Steps
To a solution of 2-aminophenol (28.55 g, 261.61 mmol) in ethanol (40 mL), was added benzaldehyde (30 mL, 31.32 g, 295.14 mmol), and this reaction mixture was refluxed for two hours, and left stirring at room temperature overnight. The creamy white precipitate was filtered, washed with ethanol and dried in vacuum oven at 80° C. for 4 hours. Giving 40.27 g (78% yields).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09437828B2 |
| Source dataset | uspto-grants-2016_09 |
| ORD ID | ord-53a7089bdb5f4d60a3967d01e364c849 |
| Source note | uspto-grants-2016_09 |