N-bromobutanimide → HCID 90449091, compound

Participants

Reaction Steps

N-(5-methylpyrazin-2-yl)-2-naphthamide (2.63 g, 10.0 mmol) was weighed and dissolved in 30 mL carbon tetrachloride. NBS (1.96 g, 11.0 mmol), BPO (242 mg, 1.0 mmol) were added and heated to reflux and reacted in dark for 12 hours. It was rotate evaporated to dryness to remove the solvent, and was used for the next step directly.

Provenance & Evidence