HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Phenylbenzene-1-sulfonyl chloride → HCID 178527497, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Phenylbenzene-1-sulfonyl chloride | HCID 3802752 | — |
| Reactant | HCID 178507542 | HCID 178507542 | — |
| Product | HCID 178527497 | HCID 178527497 | 30.2% |
Reaction Steps
The product was prepared according to General Procedure 1, described in Example 1, starting from 3-phenylbenzenesulfonylchloride (14 mg, 0.055 mmol) and 5-(3-aminophenyl)tetrazole (8 mg, 0.05 mmol) giving 5.7 mg (30%) of the title compound. 1H NMR (400 MHz, MeOH-d4) δ ppm 5.46-5.50 (m, 1 H) 7.24-7.43 (m, 5 H) 7.44-7.56 (m, 3 H) 7.70-7.79 (m, 4 H) 7.95-8.00 (m, 1 H). MS (ESI+) calcd for C19 H15N5O2S 377.0946, found 377.0946.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09233946B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-c8ce94a7e85f43c7ae5021ac7a5245a8 |
| Source note | uspto-grants-2016_01 |