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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 589685Generated: October 30, 2026

3-Phenylbenzene-1-sulfonyl chloride → HCID 178527497, compound

https://huagongshe.com/reaction/589685

Reaction equation

Participants

RoleNameHCIDCharge
Reactant3-Phenylbenzene-1-sulfonyl chlorideHCID 3802752—
ReactantHCID 178507542HCID 178507542—
ProductHCID 178527497HCID 17852749730.2%

Reaction Steps

The product was prepared according to General Procedure 1, described in Example 1, starting from 3-phenylbenzenesulfonylchloride (14 mg, 0.055 mmol) and 5-(3-aminophenyl)tetrazole (8 mg, 0.05 mmol) giving 5.7 mg (30%) of the title compound. 1H NMR (400 MHz, MeOH-d4) δ ppm 5.46-5.50 (m, 1 H) 7.24-7.43 (m, 5 H) 7.44-7.56 (m, 3 H) 7.70-7.79 (m, 4 H) 7.95-8.00 (m, 1 H). MS (ESI+) calcd for C19 H15N5O2S 377.0946, found 377.0946.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09233946B2
Source datasetuspto-grants-2016_01
ORD IDord-c8ce94a7e85f43c7ae5021ac7a5245a8
Source noteuspto-grants-2016_01