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HRID589687

反应详情

EQUATION

反应方程式

HRID 589687 的结构方程式

REACTANTS

反应物

2
结构：O=S(=O)(Cl)c1c(Cl)cc(C(F)(F)F)cc1Cl
HCID2736869

2,6-Dichloro-4-(trifluoromethyl)benzene-1-sulfonyl chloride

C7H2Cl3F3O2S

结构：Nc1cccc(-c2nnn[nH]2)c1
HCID178507542

未命名化合物

PRODUCTS

生成物

1
结构：O=S(=O)(Nc1cccc(-c2nnn[nH]2)c1)c1c(Cl)cc(C(F)(F)F)cc1Cl
HCID178527511

未命名化合物

收率 54.8%

PROCEDURE

实验过程

The product was prepared according to General Procedure 1, described in Example 1, starting from 2,6-dichloro-4-(trifluoromethyl)benzenesulfonyl chloride (17 mg, 0.055 mmol) and 5-(3-aminophenyl)tetrazole (8 mg, 0.05 mmol) giving 12 mg (54%) of the title compound. MS (ESI+) calcd for C14H8Cl2F3N5O2S 436.972785, found 436.973025.

WORKUP

后处理

  1. customThe product was prepared