HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,6-Dichloro-4-(trifluoromethyl)benzenesulfonyl chloride → 2,6-Dichloro-N-[3-(1H-tetrazol-5-yl)phenyl]-4-(trifluoromethyl)benzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,6-Dichloro-4-(trifluoromethyl)benzenesulfonyl chloride | HCID 2736869 | — |
| Reactant | HCID 178507542 | HCID 178507542 | — |
| Product | 2,6-Dichloro-N-[3-(1H-tetrazol-5-yl)phenyl]-4-(trifluoromethyl)benzenesulfonamide | HCID 178527511 | 54.8% |
Reaction Steps
The product was prepared according to General Procedure 1, described in Example 1, starting from 2,6-dichloro-4-(trifluoromethyl)benzenesulfonyl chloride (17 mg, 0.055 mmol) and 5-(3-aminophenyl)tetrazole (8 mg, 0.05 mmol) giving 12 mg (54%) of the title compound. MS (ESI+) calcd for C14H8Cl2F3N5O2S 436.972785, found 436.973025.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09233946B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-a34b450522ba45bbbd6a0c3238f5f9b4 |
| Source note | uspto-grants-2016_01 |