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HRID589690

反应详情

EQUATION

反应方程式

HRID 589690 的结构方程式

REACTANTS

反应物

2
结构：CSc1nccc(-c2ccc(S(=O)(=O)Cl)s2)n1
HCID2736995

5-[2-(Methylthio)pyrimidin-4-yl]thiophene-2-sulfonyl chloride

C9H7ClN2O2S3

结构：Nc1cccc(-c2nnn[nH]2)c1
HCID178507542

未命名化合物

PRODUCTS

生成物

1
结构：CSc1nccc(-c2ccc(S(=O)(=O)Nc3cccc(-c4nnn[nH]4)c3)s2)n1
HCID178503418

未命名化合物

收率 43.1%

PROCEDURE

实验过程

The product was prepared according to General Procedure 1, described in Example 1, starting from 5-[2-(methylthio)pyrimidin-4-yl]thiophene-2-sulfonyl chloride (17 mg, 0.055 mmol) and 5-(3-aminophenyl)tetrazole (8 mg, 0.05 mmol) giving 9.3 mg (43%) of the title compound. MS (ESI+) calcd for C16H13N7O2S3 431.029285, found 431.029205.

WORKUP

后处理

  1. customThe product was prepared