HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-(2-(Methylthio)-4-pyrimidinyl)-2-thiophenesulfonyl chloride → HCID 178503418, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-(2-(Methylthio)-4-pyrimidinyl)-2-thiophenesulfonyl chloride | HCID 2736995 | — |
| Reactant | HCID 178507542 | HCID 178507542 | — |
| Product | HCID 178503418 | HCID 178503418 | 43.1% |
Reaction Steps
The product was prepared according to General Procedure 1, described in Example 1, starting from 5-[2-(methylthio)pyrimidin-4-yl]thiophene-2-sulfonyl chloride (17 mg, 0.055 mmol) and 5-(3-aminophenyl)tetrazole (8 mg, 0.05 mmol) giving 9.3 mg (43%) of the title compound. MS (ESI+) calcd for C16H13N7O2S3 431.029285, found 431.029205.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09233946B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-67db9d71143b4fb6b32630acadb2cfd4 |
| Source note | uspto-grants-2016_01 |