HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Methoxy-3-methylbenzo[b]thiophene-2-sulfonyl chloride → HCID 178488277, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Methoxy-3-methylbenzo[b]thiophene-2-sulfonyl chloride | HCID 57440339 | — |
| Reactant | HCID 178507542 | HCID 178507542 | — |
| Product | HCID 178488277 | HCID 178488277 | 44.2% |
Reaction Steps
The product was prepared according to General Procedure 1, described in Example 1, starting from 5-methoxy-3-methylbenzothiophene-2-sulfonyl chloride (Intermediate 8) (42 mg, 0.15 mmol) and 5-(3-amino-phenyl)tetrazole (49 mg, 0.30 mmol) giving 26.6 mg (44%) of the title compound. MS (ESI+) calcd for C17H15N5O3S2 401.061631, found 401.062391.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09233946B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-f74e55260d1e4d9fb40b07cf90f7e33e |
| Source note | uspto-grants-2016_01 |