HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Aminobenzoic Acid → HCID 56941310, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Aminobenzoic Acid | HCID 7419 | — |
| Reactant | 7-Chloro-3-methylbenzo[b]thiophene-2-sulfonyl chloride | HCID 58713149 | — |
| Product | HCID 56941310 | HCID 56941310 | 63% |
Reaction Steps
The product was prepared according to General Procedure 1, described in Example 1, starting from 7-chloro-3-methylbenzothiophene-2-sulfonyl chloride (Intermediate 6) (30 mg, 0.10 mmol) and 3-amino-benzoic acid (29 mg, 0.21 mmol) to afford 24 mg (63%) of the title compound. MS (ESI+) calcd for C16H12ClNO4S2 380.989627, found 380.989977.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09233946B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-11696eb75131445f8527ab99d30b545e |
| Source note | uspto-grants-2016_01 |