HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium Hydroxide → HCID 56941312, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium Hydroxide | HCID 3939 | — |
| Reactant | HCID 66799791 | HCID 66799791 | — |
| Product | HCID 56941312 | HCID 56941312 | 7% |
Reaction Steps
The ethyl 3-{[(5-amino-3-methyl-1-benzothien-2-yl)sulfonyl]-amino}benzoate was hydrolyzed with LiOH following the hydrolysis procedure described in Example 46. The title compound was obtained in 7% yield (over two steps, 2.6 mg). MS (ESI+) calcd for C16H14N2O4S2 362.039498, found 362.040938.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09233946B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-3701e103bc544ccc9005ce283e5c63cb |
| Source note | uspto-grants-2016_01 |