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HRID589731

反应详情

EQUATION

反应方程式

HRID 589731 的结构方程式

REACTANTS

反应物

2
结构：Nc1cccc(C(=O)O)c1
HCID7419

3-Aminobenzoic Acid

C7H7NO2

结构：CSc1nccc(-c2ccc(S(=O)(=O)Cl)s2)n1
HCID2736995

5-[2-(Methylthio)pyrimidin-4-yl]thiophene-2-sulfonyl chloride

C9H7ClN2O2S3

PRODUCTS

生成物

1
结构：CSc1nccc(-c2ccc(S(=O)(=O)Nc3cccc(C(=O)O)c3)s2)n1
HCID66799915

未命名化合物

收率 78.5%

PROCEDURE

实验过程

The product was prepared according to General Procedure 1, described in Example 1, starting with 5-[2-(methylthio)pyrimidin-4-yl]thiophene-2-sulfonyl chloride (16.8 mg, 0.055 mmol) and 3-aminobenzoic acid (6.9 mg, 0.05 mmol) affording 16.0 mg (78%) of the title compound. MS (ESI+) calcd for C16H13N3O4S3 407.006818, found 407.007148.

WORKUP

后处理

  1. customThe product was prepared