HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4,6-Trichlorobenzenesulfonyl chloride → HCID 178527512, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4,6-Trichlorobenzenesulfonyl chloride | HCID 521335 | — |
| Reactant | HCID 178507542 | HCID 178507542 | — |
| Product | HCID 178527512 | HCID 178527512 | 51% |
Reaction Steps
The product was prepared according to General Procedure 6, described in Example 65, with 2,4,6-trichlorobenzenesulfonyl chloride (15.4 mg, 0.055 mmol) and 5-(3-aminophenyl)tetrazole (8.0 mg, 0.050 mmol). The title compound was obtained in 51% yield (10.7 mg). MS (ESI+) calcd mass for C13H8Cl3N5O2S 402.946428, found 402.946218.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09233946B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-c7392814e1614287b4b9363ce57fdd7f |
| Source note | uspto-grants-2016_01 |