HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,3-Dichlorobenzene-1-sulfonyl chloride → HCID 178527502, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,3-Dichlorobenzene-1-sulfonyl chloride | HCID 2734222 | — |
| Reactant | HCID 178507542 | HCID 178507542 | — |
| Product | HCID 178527502 | HCID 178527502 | 74% |
Reaction Steps
The product was prepared according to General Procedure 6, described in Example 65, with 2,3-dichlorobenzenesulfonyl chloride (13.5 mg, 0.055 mmol) and 5-(3-aminophenyl)tetrazole (8.0 mg, 0.050 mmol). The title compound was obtained in 74% yield (13.7 mg). MS (ESI+) calcd mass for C13H9Cl2N5O2S 368.985401, found 368.984901.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09233946B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-b90f3b1befd84dc2991beb6a8ca42ac3 |
| Source note | uspto-grants-2016_01 |