HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,5-Dichlorobenzenesulfonyl chloride → HCID 178527508, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,5-Dichlorobenzenesulfonyl chloride | HCID 79401 | — |
| Reactant | HCID 178507542 | HCID 178507542 | — |
| Product | HCID 178527508 | HCID 178527508 | 45% |
Reaction Steps
The product was prepared according to General Procedure 6, described in Example 65, with 2,5-dichlorobenzenesulfonyl chloride (13.5 mg, 0.055 mmol) and 5-(3-aminophenyl)tetrazole (8.0 mg, 0.050 mmol). The title compound was obtained in 45% yield (8.3 mg). MS (ESI+) calcd mass for C13H9Cl2N5O2S 368.985401, found 368.985761.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09233946B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-082e63f2f6ca405785e163f0f39d5066 |
| Source note | uspto-grants-2016_01 |