HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chloro-2-methylbenzenesulfonyl chloride → HCID 178427916, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chloro-2-methylbenzenesulfonyl chloride | HCID 522734 | — |
| Reactant | HCID 178507542 | HCID 178507542 | — |
| Product | HCID 178427916 | HCID 178427916 | 58% |
Reaction Steps
The product was prepared according to General Procedure 6, described in Example 65, with 3-chloro-2-methylbenzenesulfonyl chloride (12.4 mg, 0.055 mmol) and 5-(3-aminophenyl)tetrazole (8.0 mg, 0.050 mmol). The title compound was obtained in 58% yield (10.1 mg). MS (ESI+) calcd mass for C14H12ClN5O2S 349.040023, found 349.040413.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09233946B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-f741b6357e4944eb940b0b8423b03726 |
| Source note | uspto-grants-2016_01 |