HuagongsheHuagongshe Chemistry Print Report · For research reference only
7-Chloro-2,1,3-benzoxadiazole-4-sulfonyl chloride → HCID 178527503, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 7-Chloro-2,1,3-benzoxadiazole-4-sulfonyl chloride | HCID 612515 | — |
| Reactant | HCID 178507542 | HCID 178507542 | — |
| Product | HCID 178527503 | HCID 178527503 | 52% |
Reaction Steps
The product was prepared according to General Procedure 6, described in Example 65, with 4-chloro-7-chlorosulfonyl-2,1,3-benzoxadiazole (13.9 mg, 0.055 mmol) and 5-(3-aminophenyl)tetrazole (8.0 mg, 0.050 mmol). The title compound was obtained in 52% yield (9.8 mg). MS (ESI+) calcd mass for C13H8ClN7O3S 377.009786, found 377.010126.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09233946B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-6281a7f6ac884c3aa4f1bb83a51f821b |
| Source note | uspto-grants-2016_01 |